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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 190, 2015 - Issue 5-6: 20th International Conference on Phosphorus Chemistry (ICPC-2014)
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Original Articles

Synthesis and Crystal Structure of 2-Substituted 3-Aryl-2-Oxophenylbenzo[E]-1,4,2-Oxazaphosphinanes

Mudaris DimukhametovA.E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Kazan, 420088, Russia
,
Natalya BelovaA.E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Kazan, 420088, Russia
,
Vladimir MironovA.E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Kazan, 420088, RussiaCorrespondence[email protected]
,
Ekaterina MironovaA.E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Kazan, 420088, Russia
,
Dmitry KrivolapovA.E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Kazan, 420088, Russia
,
Petro Onys’koInstitute of Organic Chemistry, National Academy of Sciences of Ukraine, Murmanskaya Str. 5, Kiev, 02094, Ukraine
&
Yulia RassukanayaInstitute of Organic Chemistry, National Academy of Sciences of Ukraine, Murmanskaya Str. 5, Kiev, 02094, Ukraine
 show all
Pages 943-946 | Received 19 Aug 2014, Accepted 23 Nov 2014, Published online: 01 Jul 2015
 
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GRAPHICAL ABSTRACT

Abstract

Stereoisomers of 2-substituted 3-aryl-2-oxobenzo[e]-1,4,2-oxazaphosphinane derivatives were obtained by the phosphorylation of 2-arylideneaminophenols with dichlorophenylphosphine in the presence of triethylamine followed by the water treatment, which were isolated by column chromatography as pure diastereoisomers. Their structure was determined by NMR and XRD.

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Related Research Data

First syntheses of 2-hydrogeno-2-oxo-1,4,2-oxazaphosphinanes via intramolecular esterification
Source: HAL CCSD
Diastereoselective addition of 2H-2-oxo-1,4,2-oxazaphosphinanes to aldehydes and imines.
Source: HAL CCSD
Synthesis of 2-phenoxyl-2-oxo-1,4,2-oxazaphosphinanes from a three component reaction
Source: Taylor & Francis
A convenient synthesis and spatial structure of 2-aryl-2-oxo-2-phenylbenzo[e]-1,4,2-oxazaphosphinanes
Source: Springer Science and Business Media LLC
Cyclische Ester von Phosphin- und Thiophosphinsäuren
Source: Springer Science and Business Media LLC

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