ABSTRACT
An efficient protocol was developed for the synthesis of N-sulfonylimines under environment friendly conditions. Ultrasonic energy was employed to obtain the desired products in excellent yields with high purity under solvent- and catalyst-free conditions. The synthesis of new N-sulfonylimines was accomplished from various N-sulfonamides and benzaldehyde.
The structures of the synthesized compounds are confirmed by elemental analysis as well as by 1H, 13C NMR spectral data, IR and MS.
Acknowledgments
We thank Pr. Jacques Lebreton from the University of Nantes and Dr. Zouhair Bouaziz and Pr. Marc Le Borgne from the University Claude Bernard Lyon for their help in the identification for all products in NMR and MS.