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Original Articles

Interaction of sodium pentaphospholide with dimethyl acetylenedicarboxylate—A simple route to sodium 2,3,4,5-tetra(methylcarboxy)-monophospholide

Ilya BezkishkoA.E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan, RussiaCorrespondence[email protected]

Almaz ZagidullinA.E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan, Russia

Andrey PetrovA.E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan, Russia

Vasili MiluykovA.E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan, Russia

Oleg SinyashinA.E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan, Russia

GRAPHICAL ABSTRACT

ABSTRACT

Herein, we report a simple and effective route to synthesis of sodium 2,3,4,5-tetra(methylcarboxy)-monophospholide (1) based on the reaction of NaP₅ with dimethyl acetylenedicarboxylate (DMAD).

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Funding

This work was supported by the Russian Science Foundation (project no. 14-13-00589).

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Related Research Data

Synthesis and photophysical properties of 2,3,4,5-tetraphenyl-1- n -octyl-1-monophosphole

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Interaction of sodium pentaphospholide with dimethyl acetylenedicarboxylate—A simple route to sodium 2,3,4,5-tetra(methylcarboxy)-monophospholide

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