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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 191, 2016 - Issue 11-12: 21st International Conference on Phosphorus Chemistry (ICPC-2016)
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Original Articles

New 18-membered tetrakisphosphine macrocycle and its derivatives

Lenar I. MusinA.E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan, Russian FederationCorrespondence[email protected]
,
Elvira I. MusinaA.E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan, Russian Federation
,
Dmitry B. KryvolapovA.E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan, Russian Federation
,
Andrey A. KarasikA.E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan, Russian Federation
&
Oleg G. SinyashinA.E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan, Russian Federation
Pages 1591-1592 | Received 20 Jul 2016, Accepted 20 Jul 2016, Published online: 11 Aug 2016
 
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GRAPHICAL ABSTRACT

ABSTRACT

The novel 18-membered aminomethylphosphine was obtained by the reaction of 1,4-bis(2-pyridylphosphine)butane with paraformaldehyde and 4-methylbenzylamine as RSSR-isomer. Its tetraoxide and tetragold complex were obtained by the oxidation and interaction with gold chloride respectively. According to the X-Ray data the structure of oxidized product is similar to the structure of linear tetragold complex.

Funding

This work was supported by the Russian Science Foundation (grants No. 15-13-30031).

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Related Research Data

The first representatives of tetranuclear gold(I) complexes of P,N-containing cyclophanes
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Novel representatives of 16-membered aminomethylphosphines with alkyl substituents at nitrogen and their gold(I) complexes
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