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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 191, 2016 - Issue 11-12: 21st International Conference on Phosphorus Chemistry (ICPC-2016)
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Original Articles

Reduction of phosphine oxides under green chemical conditions

Tamara KovácsDepartment of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, HungaryCorrespondence[email protected]
,
Flóra CsatlósDepartment of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
,
Anita UrbanicsDepartment of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
,
Frank UhligInstitute for Inorganic Chemistry, Graz University of Technology, Graz, Austria
&
György KeglevichDepartment of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
Pages 1597-1598 | Received 20 Jul 2016, Accepted 20 Jul 2016, Published online: 11 Aug 2016
 
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GRAPHICAL ABSTRACT

ABSTRACT

The deoxygenation of phosphine oxides was studied on a series of model reactions using an aralkylsilane, arylsilanes, diarylsilanes, a disiloxane, a polysiloxane, and a disilane under solvent-free, thermal, or microwave-assisted conditions. The deoxygenations were optimized, and the reactivity of the silanes was evaluated. User-friendly accomplishments were elaborated.

Funding

This project was supported by the Hungarian Research Development and Innovation Fund (K119202). T. Kovács is grateful for the fellowship provided by Chinoin-Sanofi.

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Related Research Data

An Approach to P=N Bond Formation: Straightforward Synthesis of Arylurea‐Derived Phosphazenes via Condensation of Ph3P=O with N‐Monosubstituted Arylureas
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