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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 191, 2016 - Issue 11-12: 21st International Conference on Phosphorus Chemistry (ICPC-2016)
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Original Articles

Electrochemical pathway to CH/PH functionalization of diphenylphosphine oxide

V.V. KhrizanforovaA.E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Centre of the Russian Academy of Sciences, Kazan, RussiaCorrespondence[email protected]
,
M.N. KhrizanforovA.E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Centre of the Russian Academy of Sciences, Kazan, Russia
,
T.V. GryaznovaA.E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Centre of the Russian Academy of Sciences, Kazan, Russia
&
Y.H. BudnikovaA.E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Centre of the Russian Academy of Sciences, Kazan, Russia
Pages 1602-1603 | Received 20 Jul 2016, Accepted 20 Jul 2016, Published online: 11 Aug 2016
 
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GRAPHICAL ABSTRACT

ABSTRACT

Electrochemical oxidative CH/PH functionalization reaction between diphenylphosphine oxide and diphenylacetylene has been performed. The yield of target cyclisation product was obtained with 76% yield after 4F of electricity was passed through the reaction mixture at 1.0 V (vs. Ag/AgCl).

Funding

This work was supported by the grant of the Russian Science Foundation No. 14-23-00016.

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