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The selective reduction and boronation of the P-phenyl phosphole oxide dimer applying BH3·SMe2 as the reagent was investigated. The optimized protocol allowing the P˭O→P→BH3 conversion at 26°C in concentrated CH2Cl2 solution could be well extended also to a series of P-alkyl phosphole oxide dimers.
This project was supported by the Hungarian Research Development and Innovation Fund (K119202).
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