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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 192, 2017 - Issue 6: Harry Hudson Special Issue
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Original Articles

Dibenzyl amino(pyren-1-yl)methyl phosphonates—Their NMR and mass spectrometry characterizations

Jarosław LewkowskiDepartment of Organic Chemistry, Faculty of Chemistry, University of Łódź, Łódź, PolandCorrespondence[email protected] [email protected]
ORCID Iconhttp://orcid.org/0000-0002-2863-2320
ORCID Icon,
Rafał KarpowiczDepartment of Organic Chemistry, Faculty of Chemistry, University of Łódź, Łódź, Poland
,
Maria Rodriguez MoyaDepartment of Organic Chemistry, Faculty of Chemistry, University of Łódź, Łódź, Poland
&
Beata PasternakDepartment of Organic Chemistry, Faculty of Chemistry, University of Łódź, Łódź, PolandCorrespondence[email protected] [email protected]
Pages 719-726 | Received 13 Feb 2017, Accepted 17 Mar 2017, Published online: 25 May 2017
 
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GRAPHICAL ABSTRACT

ABSTRACT

Structures of four chosen dibenzyl amino(pyren-2-yl)methyl phosphonates were analyzed by 1H, 13C, and 31P NMR spectroscopy using simple spectra, as well as 1H-1H and 1H-13C correlation spectra (COSY and HMQC). The ESI mass spectrometry has also been applied and interesting phenomena were observed and analyzed.

Funding

Small financial support of the Faculty of Chemistry, University of Łódź is kindly acknowledged.

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