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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 194, 2019 - Issue 4-6: Proceedings of the 2018 International Conference on Phosphorus Chemistry, ICPC-22
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Original Articles

Novel chiral diamidophosphites for asymmetric metal-catalyzed reactions

I. V. ChuchelkinChemistry Department, Ryazan State University, Ryazan, Russian FederationCorrespondence[email protected]
ORCID Iconhttp://orcid.org/0000-0002-3656-468XView further author information
ORCID Icon,
V. K. GavrilovChemistry Department, Ryazan State University, Ryazan, Russian FederationView further author information
,
V. S. ZimarevChemistry Department, Ryazan State University, Ryazan, Russian FederationView further author information
,
I. D. FirsinChemistry Department, Ryazan State University, Ryazan, Russian FederationView further author information
,
M. G. MaksimovaChemistry Department, Ryazan State University, Ryazan, Russian FederationView further author information
,
A. A. ShiryaevChemistry Department, Ryazan State University, Ryazan, Russian FederationView further author information
,
S. V. ZheglovChemistry Department, Ryazan State University, Ryazan, Russian FederationView further author information
&
K. N. GavrilovChemistry Department, Ryazan State University, Ryazan, Russian FederationView further author information
 show all
Pages 455-456 | Received 13 Sep 2018, Accepted 17 Oct 2018, Published online: 20 Feb 2019
 
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Abstract

Chiral diamidophosphites with 1,3,2-diazaphospholidine cycles were prepared. A study of these chiral inducers showed them to provide up to 97% ee in the Pd-catalyzed allylic alkylation of (E)-1,3-diphenylallyl acetate with dimethyl malonate.

Graphical Abstract

Additional information

Funding

This reported study was financially supported by the Russian Science Foundation (Grant 17-73-10356, compound 3a) and Ministry of Education and Science of Russian Federation (research Project No. 4.9515.2017, compound 3b).

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