http://orcid.org/0000-0002-6791-9973
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Abstract
Structures of the individual compound 2-(2-(diphenylphosphoryl)acetyl)-N-phenylhydrazinecarbothioamide and its solvate with DMSO were determined by the single X-ray analysis. Despite the lability of the system, in crystals of two modifications the similar conformation of the molecule is realized. In the crystals of individual thiosemicarbazide and its solvate form 1 D supramolecular structures, but the crystal packing of them is distinguished significantly. Solvent molecules are located in the 0D-voids in the crystals.
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Funding
The Synthetic part of work was supported by the Russian Science Foundation (project no. 14-23-00073-p), crystallographic part was supported by the Russian Foundation for Basic Research (grant No 18-33-00228).