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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 194, 2019 - Issue 4-6: Proceedings of the 2018 International Conference on Phosphorus Chemistry, ICPC-22
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Short Communication

The reaction of phosphorylation of trans-aconitic acid by tertiary phosphines

Yulia V. BakhtiyarovaKazan Federal University, Kazan, Russia; Correspondence[email protected]
ORCID Iconhttp://orcid.org/0000-0002-1865-274XView further author information
ORCID Icon,
Alfiya F. AksunovaKazan Federal University, Kazan, Russia; View further author information
,
Semyon R. RomanovKazan Federal University, Kazan, Russia; View further author information
,
Dmitry I. BakhtiyarovKazan Federal University, Kazan, Russia; View further author information
,
Kamil A. IvshinKazan Federal University, Kazan, Russia; View further author information
,
Olga N. KataevaKazan Federal University, Kazan, Russia; ;A. E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Kazan, RussiaView further author information
,
Svetlana N. EgorovaKazan State Medical University, Kazan, Russia; View further author information
,
Irina V. GalkinaKazan Federal University, Kazan, Russia; View further author information
&
Vladimir I. GalkinKazan Federal University, Kazan, Russia; View further author information
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Pages 319-320 | Received 24 Sep 2018, Accepted 10 Oct 2018, Published online: 22 Nov 2018
 
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Abstract

New stable carboxylate phosphabetaines were synthesized by the phosphorylation of trans-aconitic acid by tertiary phosphines. The structures of the isolated compounds were determined by NMR spectroscopy, X-ray single crystal diffraction studies and elemental analysis.

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Additional information

Funding

This work was funded by the subsidy allocated to Kazan Federal University for the state assignment in the sphere of scientific activities (No 4.5888.2017/8.9).

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Related Research Data

CCDC 1865984: Experimental Crystal Structure Determination
Source: Cambridge Crystallographic Data Centre
Phosphabetaines on the Basis of Triphenylphosphine and Unsaturated Dicarboxylic Acids
Source: Informa UK Limited
Synthesis of carboxylate phosphabetaines from 3-(diphenylphosphino)propanoic acid and unsaturated monocarboxylic acids
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The Influence of Solvents on the Alkylation of Carboxylate Phosphabetaines with Alkyl Iodides
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The synthesis and reactions of betaines formed in reactions of tertiary phosphines with unsaturated carboxylic acids and their derivatives
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Synthesis, structure, and biological activity of dicarboxylate phosphabetaines
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