http://orcid.org/0000-0003-4029-6777, , http://orcid.org/0000-0002-1979-6913, , http://orcid.org/0000-0002-4029-9874 & ![Sample our Physical Sciences journals, sign in here to start your FREE access for 14 days]({"type":"image" , "src" : "/sda/110819/TOC-Subject-Sample-2021-Physical-Sciences.jpg"})
A convenient and generalizable procedure has been optimized to access to 1-hydroxymethylene-1,1-bisphosphinate compounds. Several alkyl, including an alendronate bisphosphinate analog, and (hetero)aryl compounds were rapidly obtained in satisfying to excellent yields. A side product could be identified as a phosphino-phosphonate isomer and plausible mechanistic pathways are discussed here.
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