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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 197, 2022 - Issue 5-6: ICPC-23: 23rd International Conference on Phosphorus Chemistry; Guest Editors:Professor Jozef Drabowicz; Professor Piotr Kiełbasiński and Professor Tomasz Cierpiał
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Articles

New intramolecular cyclization of 2H-benzo[e]-1,2-oxaphosphorinine derivatives—a way to the synthesis of unsymmetrical cage phosphonates

A. V. Zalaltdinovaa Arbuzov Institute of Organic and Physical Chemistry, FRC Kazan Scientific Center of RAS, Kazan, RussiaCorrespondence[email protected]
ORCID Iconhttps://orcid.org/0000-0002-4822-7330View further author information
ORCID Icon,
Yu. M. Sadykovaa Arbuzov Institute of Organic and Physical Chemistry, FRC Kazan Scientific Center of RAS, Kazan, RussiaORCID Iconhttps://orcid.org/0000-0003-2093-2860View further author information
ORCID Icon,
A. K. Smailovb Kazan National Research Technological University, Kazan, RussiaView further author information
,
L. M. Trofimovac Chuvash State University named after I.N. Ulyanov, Cheboksary, RussiaView further author information
,
A. R. Burilova Arbuzov Institute of Organic and Physical Chemistry, FRC Kazan Scientific Center of RAS, Kazan, RussiaView further author information
&
M. A. Pudovika Arbuzov Institute of Organic and Physical Chemistry, FRC Kazan Scientific Center of RAS, Kazan, RussiaView further author information
Pages 549-550 | Received 14 Oct 2021, Accepted 28 Oct 2021, Published online: 29 Nov 2021
 
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Abstract

A new approach has been developed to obtain 2H-1,2-oxaphosphorinine, which is a platform for the synthesis of asymmetric cage phosphonates. The structures of the obtained products were confirmed by IR spectroscopy, 1H, 13C NMR spectroscopy, and X-ray structural analysis.

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Funding

This work was supported by the Russian Foundation for the Basic research (grant no 20-03-00118).

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