UNUSUAL TRIPOD-LIKE LIGANDS. SYNTHESIS OF 2,2-BIS(DIPHENYLPHOSPHINOMETHYL)-1-METHOXYPROPANE AND 2,2-BIS(PHENYLTHIOMETHYL)-1-METHOXYPROPANE

Shiuh-Tzung Liu Department of Chemistry, National Taiwan University, Taipei, Taiwan R.O.C., 10764

Chien-Hung Yieh Department of Chemistry, National Taiwan University, Taipei, Taiwan R.O.C., 10764

Hui-Jane Lu Department of Chemistry, National Taiwan University, Taipei, Taiwan R.O.C., 10764

Abstract

By employment of 1,1,1-tris(hydroxymethyl)ethane as the starting material, syntheses of two novel tripod-like terdentates with mixed donor properties, 2,2-Bis(diphenylphosphinomethyl)-1-methoxypropane (P₂O) and 2,2-Bis(diphenylphosphinomethyl)-1-methoxypropane (S₂O) are reported. Structural confirmation is based on spectroscopic and analytical results.

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UNUSUAL TRIPOD-LIKE LIGANDS. SYNTHESIS OF 2,2-BIS(DIPHENYLPHOSPHINOMETHYL)-1-METHOXYPROPANE AND 2,2-BIS(PHENYLTHIOMETHYL)-1-METHOXYPROPANE

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UNUSUAL TRIPOD-LIKE LIGANDS. SYNTHESIS OF 2,2-BIS(DIPHENYLPHOSPHINOMETHYL)-1-METHOXYPROPANE AND 2,2-BIS(PHENYLTHIOMETHYL)-1-METHOXYPROPANE

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