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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 49-50, 1990 - Issue 1-4
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Section 2: Chemistry of Phosphorus Compounds in Particular Coordination Bonding

Synthesis and Reactivity of the First Stable λ5-Phosphaacetylene

Guy Bertrand Laboratoire de Chimie de Coordination du CNRS, 205, route de Narbonne, 31077, Toulouse Cédex, France
,
Alain Igau Laboratoire de Chimie de Coordination du CNRS, 205, route de Narbonne, 31077, Toulouse Cédex, France
,
Antoine Baceireco Laboratoire de Chimie de Coordination du CNRS, 205, route de Narbonne, 31077, Toulouse Cédex, France
&
Hansjorg Grutzmacher Laboratoire de Chimie de Coordination du CNRS, 205, route de Narbonne, 31077, Toulouse Cédex, France
Pages 301-304 | Published online: 04 Oct 2006
 
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Abstract

The synthesis and reactivity of he P-bis(diisopropylamino) trimethylsilylphosphaacetylene (bp 75–80°C/10−2) is reported. Addition of trimethylsilyltriflate to this compound leads to a stable methylenephosphonium salt which has been characterized by an X-ray diffraction study.

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