The 1,3-dithiane ring undergoes cleavage even under mild neutral reaction conditions when heated in the presence of trifluoromethylthiocopper. The free-radical nature of the reaction was confirmed by the characterization of bis-(trifluoromethyl)disulfide as one of the products.
Reaction of 1,3-Dithiane with Trifluoromethylthiocopper
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