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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 69, 1992 - Issue 3-4
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Original Articles

NITROGEN-CONTAINING TRIPODAL PHOSPHINE LIGANDS

Hsing-Ell Wang Department of Chemistry, National Taiwan University, Taipei, Taiwan, 107, R.O.C.
,
Chung-Yuan Liu Department of Chemistry, National Taiwan University, Taipei, Taiwan, 107, R.O.C.
,
Ming-Chu Cheng Department of Chemistry, National Taiwan University, Taipei, Taiwan, 107, R.O.C.
,
Shie-Ming Peng Department of Chemistry, National Taiwan University, Taipei, Taiwan, 107, R.O.C.
&
Shiuh-Tzung Liu Department of Chemistry, National Taiwan University, Taipei, Taiwan, 107, R.O.C.
Pages 201-211 | Received 01 Jan 1992, Accepted 09 Mar 1992, Published online: 04 Oct 2006
 
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Abstract

Two tripodal phosphine ligands, 2,2-bis(diphenylphosphinomethyl)-1-(diethylamino)propane (P2N) and 2,2-bis(diethylaminomethyl)-1-diphenylphosphinopropane (PN2) were synthesized. Palladium(II) and Platinum(II) complexes with these ligands were obtained from the reaction of PdCl2(CH3CN)2 and K2PtCl4 respectively. Complex (P2N)PtCl2 crystallizes in space group Pca21 with a = 21.983(5), b = 11.419(1), c = 14.179(3) Å, and the structure was refined to R = 0.039 by using 2826 reflections.

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