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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 80, 1993 - Issue 1-4
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COMMUNICATION

SELENOBENZOPHENONES AND DIAZOALKANES: REACTION AND MECHANISTIC ELUCIDATION

Kentaro Okuma Department of Chemistry, Faculty of Science, Fukuoka University, Jonan-ku, Fukuoka, 814-01, Japan
,
Kazuki Kojima Department of Chemistry, Faculty of Science, Fukuoka University, Jonan-ku, Fukuoka, 814-01, Japan
&
Hiroshi Ohta Department of Chemistry, Faculty of Science, Fukuoka University, Jonan-ku, Fukuoka, 814-01, Japan
Pages 259-262 | Received 10 Dec 1992, Accepted 22 Feb 1993, Published online: 23 Sep 2006
 
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Abstract

The reaction of selenobenzophenones with diazomethane afforded the corresponding diarylethylenes and symmetrical olefins. The reaction with other diazoalkanes gave three different types of olefins. This reaction proceeded through selenadiazoline intermediates and retrocyclization was observed.

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Related Research Data

Synthesis of Δ3‐1,3,4‐Telluradiazolines by Reaction of Fenchone Hydrazone with Tellurium Tetrachloride: Mechanistic Insight into Twofold Extrusion
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