The Preparation of Per-Deuterated Aromatic Hydrocarbons Using Organosulfur Compounds: Phosphorus, Sulfur, and Silicon and the Related Elements: Vol 74, No 1-4

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Abstract

Per-deuteration of benzothiophene (1), benzenethiol (2) and p-methylbenzenethiol (3) has been accomplished by reaction with D₂O containing dissolved metal salts at 250° – 315°C. Desulfurization of the products gave per-deutero ethylbenzene, benzene and toluene in high overall yield (> 95%).

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The Preparation of Per-Deuterated Aromatic Hydrocarbons Using Organosulfur Compounds

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The Preparation of Per-Deuterated Aromatic Hydrocarbons Using Organosulfur Compounds

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