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The metallacycles , W have been studied in CH2Cl2 using cyclic voltammetry. The observed redox potentials indicate that the cyclic π-base ligand, [NPPh2NPPh2N]3−, is capable of stabilising high oxidation states in both molybdenum and tungsten complexes. Empirical MO calculations are presented which rationalize the electronic structure of the metallacycles.
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