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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 106, 1995 - Issue 1-4
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Original Articles

ORGANOSULPHUR PHOSPHORUS ACID COMPOUNDS. PART 6. PREPARATION AND ANALYTICAL IDENTIFICATION OF FLUOROBENZYLPHOSPHONO-DISULPHONIC ACIDS

E. Montoner Dipartimento di Chimica Generale ed Organica Applicata, Universitá di Torino, Corso Massimo D'Azeglio, 48-10125, Torino, Italy
,
P. Savarino Dipartimento di Chimica Generale ed Organica Applicata, Universitá di Torino, Corso Massimo D'Azeglio, 48-10125, Torino, Italy
,
F. Adani Dipartimento di Fisiologia delle Piante Coltivate e Chimica Agraria, Universitá di Milano, Via Celoria, 2-20133, Milano, Italy
&
G. Ricca Dipartimento di Chimica Organica e Industriale, Universitá di Milano, Via Venezian, 21-20133, Milano, Italy
Pages 37-45 | Received 28 Mar 1995, Published online: 24 Sep 2006
 
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Abstract

Three new organosulphur phosphorus acid compounds have been obtained by sulphonation with liquid SO3: 2-fluorobenzylphosphonic gave 2-fluorobenzylphosphono-3,5-disulphonic, 3-fluorobenzylphosphonic acid gave 3-fluorobenzylphosphono-4,6-disulphonic acid, and 4-fluorobenzylphosphonic acid gave 4-fluorobenzylphosphono-3,5-disulphonic acid in nearly quantitative yields. The products analysis is based on n.m.r. spectroscopy.

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