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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 106, 1995 - Issue 1-4
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Original Articles

STUDY ON THE SYNTHESIS OF THE ELECTRON DONOR MOLECULE OF [BIS(ETHYLENEDITHIO)-TETRATHIAFULVALENE] (BEDT-TTF)

Sheng-Gao Liu Institute of Chemistry, Academia Sinica, Beijing, 100080, P. R. of China
,
Pei-Ji Wu Institute of Chemistry, Academia Sinica, Beijing, 100080, P. R. of China
,
Yun-Qi Liu Institute of Chemistry, Academia Sinica, Beijing, 100080, P. R. of China
&
Dao-Ben Zhu Institute of Chemistry, Academia Sinica, Beijing, 100080, P. R. of China
Pages 145-153 | Received 08 Apr 1995, Accepted 24 May 1995, Published online: 24 Sep 2006
 
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Abstract

Two kinds of synthetic methods for the organic donor molecule BEDT-TTF or ET [bis(ethylenedithio)-tetrathiafulvalene] are reviewed and compared. Through detailed and systematic studies of the synthesis of BEDT-TTF, a convenient, reliable, ready and high-yield synthetic procedure is presented, which is superior to the methods reported to date in terms of the yield and reproducibility.

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Related Research Data

Neutral coordination polymers based on a metal–mono(dithiolene) complex: synthesis, crystal structure and supramolecular chemistry of [Zn(dmit)(4,4′-bpy)]n, [Zn(dmit)(4,4′-bpe)]n and [Zn(dmit)(bix)]n (4,4′-bpy = 4,4′-bipyridine, 4,4′-bpe = trans-1,2-bis(4-pyridyl)ethene, bix = 1,4-bis(imidazole-1-ylmethyl)-benzene
Source: Royal Society of Chemistry (RSC)

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