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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 101, 1995 - Issue 1-4
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Original Articles

SYNTHESIS OF METAL SILICIDE POWDERS BY THERMOLYSIS OF METAL CHLORIDES WITH MAGNESIUM SILICIDE

Jonathan C. Fitzmaurice Department of Chemistry, Christopher Ingold Laboratories, University College London, 20 Gordon Street, London, WC1H 0AJ, United Kingdom
,
Andrew L. Hector Department of Chemistry, Christopher Ingold Laboratories, University College London, 20 Gordon Street, London, WC1H 0AJ, United Kingdom
,
Ivan P. Parkin Department of Chemistry, Christopher Ingold Laboratories, University College London, 20 Gordon Street, London, WC1H 0AJ, United Kingdom
&
Adrian T. Rowley Department of Chemistry, Christopher Ingold Laboratories, University College London, 20 Gordon Street, London, WC1H 0AJ, United Kingdom
Pages 47-55 | Received 23 May 1994, Accepted 09 Nov 1994, Published online: 04 Oct 2006
 
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Abstract

Thermolysis (850°C) of a mixture of Mg2Si and MCl13, (M = Y, Gd, Dy, Ho, Ti, Zr, Hf, Nb, Ta, Mo, W, Fe, Pt; n = 3, 4, 5) produces metal silicides MxSiy as microcrystalline powders. The reactions give a useful insight into the mechanisms working in this type of reaction.

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Related Research Data

Transition metal silicides: fundamentals, preparation and catalytic applications
Source: Royal Society of Chemistry (RSC)

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