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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 113, 1996 - Issue 1-4
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Communication

A CONVENIENT DIRECT SYNTHESIS OF α-N,N-DIALKYLAMINOPHOSPHONATES UNDER APROTIC CONDITIONS

Catherine Malhiac Laboratoire d'Hétérochimie Organique (IRCOF), Université de Rouen, F-76821, Mont Saint Aignan, Cedex, France
,
Jean-Claude Combret Laboratoire d'Hétérochimie Organique (IRCOF), Université de Rouen, F-76821, Mont Saint Aignan, Cedex, France
,
Kamal Boussad Laboratoire d'Hétérochimie Organique (IRCOF), Université de Rouen, F-76821, Mont Saint Aignan, Cedex, France
&
Jean-Louis Klein Laboratoire d'Hétérochimie Organique (IRCOF), Université de Rouen, F-76821, Mont Saint Aignan, Cedex, France
Pages 299-301 | Received 09 Aug 1995, Accepted 09 Jan 1996, Published online: 04 Oct 2006
 
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Abstract

A general one-pot synthesis of N,N-dialkylaminophosphonates under aprotic conditions is proposed using aromatic, heteroaromatic or aliphatic aldehydes and N,N-dialkyl-aminosilanes under trimethylsilyltriflate catalysis.

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