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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 130, 1997 - Issue 1
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Original Articles

STUDIES OF TRIS-[(DIMETHYLBENZYLSILYL)METHYLENE]TIN MONO(DI)THIOPHOSPHATES

Hua Liu Institute of Elemento-Organic Chemistry, Nankai University, Tianjin, 300071, People's Republic of China
,
Qing-Lan Xie Institute of Elemento-Organic Chemistry, Nankai University, Tianjin, 300071, People's Republic of China
,
Songlan Li Institute of Elemento-Organic Chemistry, Nankai University, Tianjin, 300071, People's Republic of China
&
Ji-Tao Wang Institute of Elemento-Organic Chemistry, Nankai University, Tianjin, 300071, People's Republic of China
Pages 193-202 | Received 30 Jun 1997, Accepted 03 Sep 1997, Published online: 24 Sep 2006
 
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Abstract

Twenty-five new compounds of the form (PhCH2Me2SiCH2)3SnSP(X)(ORl)(OR2)(X = O:R1 =C2H5, R2 = Substituted phenyl; X = S:R1 = R2 = hydrocarbyl) have been synthesized. Their structures were characterized by IR, 1H, 119Sn, 31P NMR, MS and elemental analyses. 119Sn NMR measurement of chemical shift have shown that there is a good linear relationship of 119Sn chemical shift with para-substituent Hammett constants.

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