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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 126, 1997 - Issue 1
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Original Articles

SYNTHESES OF 1,5-BENZOTHIAZEPINES, PART XVI: SYNTHESES OF 8-ETHOXY/FLUORO-2-CABOXY-4-(FLUORINATED ARYL) -2,3-DIHYDRO-1,5-BENZOTHIAZEPINESAS PROSPECTIVE CARDIOVASCULAR AGENTS

Umesh C. Pant Department of Chemistry, University of Rajathan, Jaipur, 302 004, India
,
Mani Upreti Department of Chemistry, University of Rajathan, Jaipur, 302 004, India
,
Seema Pant Department of Chemistry, University of Rajathan, Jaipur, 302 004, India
,
Anshu Dandia Department of Chemistry, University of Rajathan, Jaipur, 302 004, India
,
G. K. Patnaik Pharmacology Division, C.D.R.I., Lucknow, 226001, India
&
A. K. Goel Department of Chemistry, University of Rajathan, Jaipur, 302 004, India
Pages 193-199 | Received 25 Nov 1996, Accepted 04 Mar 1997, Published online: 04 Oct 2006
 
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Abstract

Syntheses of fluorinated 8-ethoxy/fluoro-2-carboxy-4-substituted ary-2,3-dihydro1,5-benzothiazepines having substitutents as chloro, methyl and trifluoromethyl have been achieved by the reaction of 5-ethoxy/-fluoro-2-aminobenzenethiols with fluorinated 3-substituted benzoyl-2-propenoic acids in toluene with catalytic amount of trifluoroacetic acid. The progress of the reactions was monitored by t.1.c. studies. Structures of the title compounds are established by IR, PMR and mass spectral studies and microestimation data of nitrogen.

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Related Research Data

2-(2-ARYL-2-OXOETHYL)-4H-BENZO-1,4-THIAZIN-3-ONES AS PRODUCTS OF THE REACTION OF 2-AMINOTHIOPHENOL WITH β-AROYLACRYLIC ACIDS
Source: Informa UK Limited
Versatile three component procedure for combinatorial synthesis of biologically relevant scaffold spiro[indole-thiazolidinones] under aqueous conditions
Source: Royal Society of Chemistry (RSC)

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