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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 147, 1999 - Issue 1
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Posters

Metal-Rich Phosphanediyl-and Arsanediyl-Clusters

Klaus Merz Chair of Inorganic Chemistry I, University Bochum, D-44801, Bochum, Germany
,
Stefan Martin Chair of Inorganic Chemistry I, University Bochum, D-44801, Bochum, Germany
,
Vassili Pintchouk Chair of Inorganic Chemistry I, University Bochum, D-44801, Bochum, Germany
,
Hans Pritzkow Chair of Inorganic Chemistry I, University Bochum, D-44801, Bochum, Germany
&
Matthias Driess Chair of Inorganic Chemistry I, University Bochum, D-44801, Bochum, Germany
Page 259 | Published online: 23 Oct 2006
 
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Abstract

The reactions of primary silylphosphanes and -arsanes 1 with BuLi yield the three-dimensional M2ER-aggregates 2 (E = P, As). We observed that the double lithiation of 1 in the presence of Li2O results in the formation of the aggregates 3 and 4.

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