Simultaneous Removal of two 2-cyano-1,1-dimethylethyl Groups from Bis(2-cyano-1,1-dimethylethyl) Thymidine 3′-phosphate Derivatives by the Use of DBU/BSA

Mitsuo Sekine Department of Life Science, Faculty of Biological Sciences and Technology, Tokyo Institute of Technology Nagatsuta, Midoriku, Yokohama, 227, Japan

Hiroyuki Tsuruoka Department of Life Science, Faculty of Biological Sciences and Technology, Tokyo Institute of Technology Nagatsuta, Midoriku, Yokohama, 227, Japan

Shin Iimura Department of Life Science, Faculty of Biological Sciences and Technology, Tokyo Institute of Technology Nagatsuta, Midoriku, Yokohama, 227, Japan

Takeshi Wada Department of Life Science, Faculty of Biological Sciences and Technology, Tokyo Institute of Technology Nagatsuta, Midoriku, Yokohama, 227, Japan

Abstract

A combined reagent of DBU / bis(trimethylsilyl)acetamide (BSA) was highly effective for the simultaneous and rapid removal of two 2-cyano-1,1-dimethylethyl groups from a bis(2-cyano-1,1-dimethylethyl) thymidine 3′-phosphate derivative.

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Simultaneous Removal of two 2-cyano-1,1-dimethylethyl Groups from Bis(2-cyano-1,1-dimethylethyl) Thymidine 3′-phosphate Derivatives by the Use of DBU/BSA

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Simultaneous Removal of two 2-cyano-1,1-dimethylethyl Groups from Bis(2-cyano-1,1-dimethylethyl) Thymidine 3′-phosphate Derivatives by the Use of DBU/BSA

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