Alkoxy-derived ferroelectric PZT films: The effect of lead acetate dehydration techniques and lead content in the electrochemically prepared solutions on the properties of the films

M. I. Yanovskaya Karpov Institute of Physical Chemistry, 103064, Vorontsovo Pole, 10, Moscow, Russia

I. E. Obvintseva Karpov Institute of Physical Chemistry, 103064, Vorontsovo Pole, 10, Moscow, Russia

L. I. Solovyova NIPIM, 300600, Lenina prosp. 106-a, Tula, Russia

E. P. Kovsman NIPIM, 300600, Lenina prosp. 106-a, Tula, Russia

K. A. Vorotilov Moscow Institute of Radioengineering, Electronics and Automation, 117454, Vernadsky prosp. 78, Moscow, Russia

V. A. Vasilyev Moscow Institute of Radioengineering, Electronics and Automation, 117454, Vernadsky prosp. 78, Moscow, Russia

Abstract

Different ways of dehydration of lead acetate trihydrate for its application in sol-gel techniques are discussed. Reaction of Pb(CH₃COO)₂·3H₂O with acetic acid anhydride proved to be the most efficient way of its dehydration. Characteristics of the solutions of lead acetate in methoxyethanol dehydrated by different methods are presented. Solutions for preparation of PZT films are prepared using electrochemical dissolution of titanium and zirconium in methoxyethanol. Physico-chemical properties of these solutions alongside with structural and electrical characteristics of the PZT films obtained from these solutions are presented. The effect of lead content in solutions on the properties of the films obtained is discussed.

Key Words:

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Order Reprints Request Corporate Permissions

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

Request Academic Permissions

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.

Alkoxy-derived ferroelectric PZT films: The effect of lead acetate dehydration techniques and lead content in the electrochemically prepared solutions on the properties of the films

Information for

Open access

Opportunities

Help and information

Alkoxy-derived ferroelectric PZT films: The effect of lead acetate dehydration techniques and lead content in the electrochemically prepared solutions on the properties of the films

Abstract

Reprints and Corporate Permissions

Academic Permissions

Related research

To cite this article:

Download citation

Information for

Open access

Opportunities

Help and information

Keep up to date

Your download is now in progress and you may close this window

Login or register to access this feature