Spectroscopic Study of Silver-Containing Mesogenic Cyanobiphenyls in Solid Phase

Tatyana I. Shabatina Department of Chemistry, Moscow State University, 119899, Moscow, Russia; E-mail: [email protected]

Eugenia V. Vovk Department of Chemistry, Moscow State University, 119899, Moscow, Russia

Yurii N. Morosov Department of Chemistry, Moscow State University, 119899, Moscow, Russia

Vadim A. Timoshenko Department of Chemistry, Moscow State University, 119899, Moscow, Russia

Gleb B. Sergeev Department of Chemistry, Moscow State University, 119899, Moscow, Russia

Abstract

Silver-containing mesogenic alkylcyanobiphenils (CB): C_nH_2n+1-C₆H₅-C₆H₅-CN, where n=5 (5 CB), 7 (7 CB), and 8 (8 CB) systems were obtained by low temperature co-condensation of metal and organic component vapours. The formation of low temperature Ag-CB complexes was shown by IR-, UV-visible and ESR techniques. Thermal degradation of the complexes led to the formation of nanosize (15–30) silver particles and their further aggregation in anisotropic matrices.

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Spectroscopic Study of Silver-Containing Mesogenic Cyanobiphenyls in Solid Phase

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