Molecular Inclusion Crystals of Novel Heterocyclic Host Compounds

Kiyoshi Matsumoto Graduate School of Human and Environmental Studies, and Faculty of Integrated Human Studies, Kyoto University, Kyoto, 606-01, Japan

Mitsuo Toda Faculty of Engineering, Shizuoka University, Hamamatsu, Japan

Yukio Ikemi Graduate School of Human and Environmental Studies, and Faculty of Integrated Human Studies, Kyoto University, Kyoto, 606-01, Japan

Akikazu Kakehi Faculty of Engineering, Shinshu University, Nagano, 380, Japan

Shiro Hashimoto Graduate School of Human and Environmental Studies, and Faculty of Integrated Human Studies, Kyoto University, Kyoto, 606-01, Japan

Motoo Shiro Research Department, Rigaku Corporation, Akishima, Tokyo, 196, Japan

Shinichi Otani Graduate School of Human and Environmental Studies, and Faculty of Integrated Human Studies, Kyoto University, Kyoto, 606-01, Japan

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Abstract

Inclusion phenomena of the solvents such as hexane, benzene, and dichloromethane in either the crystals or glassy states of the armed-1,4,8,12-tetrazacyclopentadecanes were observed, whereas only few inclusion was found in the armed 1,4,8,11- tetraazacyclotetradecanes. As further examples of undesigned inclusion hosts, the 1:2 adduct, obtained by Diels-Alder reaction of [2.2]paracyclophane with 4-phenyl-1,2,4-triazoline-3,5-dione, along with the 1:2 adducts fiom 5-cyano- 1,4-diphenylpyridazino[4.5-a]- indolizines and dimethyl acetylenedicarboxylate (DMAD) are described.

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Molecular Inclusion Crystals of Novel Heterocyclic Host Compounds

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