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Fullerene Science and Technology Volume 4, 1996 - Issue 6
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Original Articles

Preparation and Characterization of Inorganic Fluorides—Fullerenes Compounds

André Hamwi Laboratoire de Chimie des Solides, Université B. Pascal Clermont-Ferrand II, 63177, Aubière, France
,
Catherine Latouche Laboratoire de Chimie des Solides, Université B. Pascal Clermont-Ferrand II, 63177, Aubière, France
,
Béatrice Burteaux Laboratoire de Chimie des Solides, Université B. Pascal Clermont-Ferrand II, 63177, Aubière, France
&
Jacques Dupuis Laboratoire des Sciences et Materiaux pour l'Electronique et d'Automatique, Université B. Pascal, Clermont Ferrand II, 63177, Aubière, France
Pages 1213-1226 | Received 26 Feb 1996, Published online: 22 Aug 2006
 
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Abstract

Reaction of metallic fluorides: WF6 TaF5, NbF5 and TiF4 with C60/C70 extract was performed at appropriate temperatures. M0F5 and BF3 fluorides do not react. Chemical formulas based on mass uptake show MFn/C60 ratios up to 2.00. Compounds were analysed by means of X-ray diffraction, FT-IR and NMR spectroscopies. The presence of neutral fluorides and associated anionic species is put forward and it is shown that MFn compounds do not act as fluorination agents. Electrical conductivity measurements are also presented.

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