Microwave-assisted extraction of phenolics from Canarium album L. and identification of the main phenolic compound

Abstract

Microwave-assisted extraction (MAE) was applied in the extraction of phenolics from Canarium album L. Effects of various conditions including the solvent, solvent to material ratio, microwave power and irradiation time on extraction yield of phenolics were investigated. In terms of the optimal conditions of MAE, it was concluded that 70% (v/v) of ethanol was the proper extraction solvent, the solvent to material ratio was 10 : 1 (mL : g), and the microwave power and irradiation time were 600 W and 15 s, respectively. Compared with normal stirring extraction and ultrasound-assisted extraction, the MAE of phenolics from C. album L. was more time efficient and gave a high extraction rate. More than 1.2% extraction yield was achieved with MAE, and the purity of the phenolics in the extract product was up to 25%. In addition, by ultraviolet-visible (UV) spectrometry and electrospray ionised mass spectrometry (ESI/MS), the main phenolic compound in the extract product was identified as gallic acid.

Keywords:

• Canarium album L.
• phenolic
• microwave
• extraction
• ESI/MS

Acknowledgements

This work was financially supported by the Agricultural Transformation Fund Program of Scientific and Technical Achievement from the Ministry of Science and Technology, P.R. China (No. 03EFN217100327). The authors are very grateful for the assistance of Shangwei Cheng, Guanjun Tao and Fang Qin of the Analysis Center, Jiangnan University, Wuxi, China.