Nucleation of dislocations during nanoindentation in MgO

Abstract

This study investigates the incipient plasticity during a nanoindentation test with a spherical indenter in magnesium oxide single crystals. The load–displacement curves show multiple pop-ins, interspaced by elastic deformation, and reveal the transition from an initial elastic deformation regime to a continuous elastoplastic one. Nanoindentations have been stopped after the first pop-in and the dislocation structures have been three-dimensionally characterized by AFM observations of the surface deformation and by nanoetching. The dislocation pattern shows two activated slip systems. The resolved shear stress has been calculated just before the pop-in, for all of the activated slip systems. The final positions of the dislocations generated during the first pop-in reveal that they were all nucleated at the point of maximum resolved shear stress.

Notes

‡Current address: Dpto. Ciencia de los Materiales e Ingeniería Metalúrgica, Universitat Politècnica de Catalunya, ETSEIB, Avda. Diagonal 647, 08028 Barcelona, Spain.

Additional information

Notes on contributors

Y. Gaillard‡

‡Current address: Dpto. Ciencia de los Materiales e Ingeniería Metalúrgica, Universitat Politècnica de Catalunya, ETSEIB, Avda. Diagonal 647, 08028 Barcelona, Spain.