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Part A: Materials Science

Study of vacancy defects and their thermal stability in MeV Fe ion irradiated RAFM steel using positron beam Doppler broadening spectroscopy

ORCID Icon, , , , , , , & show all
Pages 38-54 | Received 11 Jan 2018, Accepted 10 Sep 2018, Published online: 03 Oct 2018
 

ABSTRACT

Indian reduced activation ferritic-martensitic steel was irradiated with 1.1 MeV Fe ions to various doses from 1 to100 dpa at room temperature. The depth profiling of irradiation-induced vacancy-type defects and the defect-recovery under post-irradiation annealing was studied using variable low-energy positron beam Doppler broadening spectroscopy. The influence of irradiation-induced defects on the microstructural properties was studied by glancing incidence x-ray diffraction (GIXRD) and nanoindentation technique. Positron annihilation study showed the signatures of reduced vacancy concentration at the peak damage region due to injected interstitial effect from 30 to 100 dpa and the widening of vacancy-interstitial recombination-rich region towards the end of ion range with the increase in dose. The GIXRD results were analysed by modified Williamson–Hall plot method, and the variation of coherent domain size and micro-strain with irradiation dose was studied. Irradiation-induced hardening was observed in the nanoindentation study. The features observed in the GIXRD and nanoindentation study are correlated with the depth-resolved defect distribution observed in the positron annihilation study.

Acknowledgements

The authors acknowledge Dr. K. Laha, Materials and Metallurgy group, IGCAR for providing the samples.

Disclosure statement

No potential conflict of interest was reported by the authors.

ORCID

Renjith Ramachandran http://orcid.org/0000-0001-5670-0952

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