A Convenient Method for the Synthesis of ATP and Ap₄A

Koichiro Fukuoka Department of Life Chemistry, Tokyo Institute of Technology, Nagatsuta, Midoriku, Yokohama, 227, Japan

Fuminori Suda Department of Life Chemistry, Tokyo Institute of Technology, Nagatsuta, Midoriku, Yokohama, 227, Japan

Masahide Ishikawa Department of Life Chemistry, Tokyo Institute of Technology, Nagatsuta, Midoriku, Yokohama, 227, Japan

Tsujiaki Hata Department of Life Chemistry, Tokyo Institute of Technology, Nagatsuta, Midoriku, Yokohama, 227, Japan

Abstract

A bifunctional phosphorylating reagent, O-8-(5-chloroquinolyl) S-phenyl phosphorothioate (1) was employed for the synthesis of adenosine 5′-triphosphate (ATP) and diadenosine 5′-tetraphosphate (Ap₄A) from adenosine 5′-phosphate (AMP) on a large scale.

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A Convenient Method for the Synthesis of ATP and Ap₄A