Supercritical Carbon Dioxide‐Soluble Fluorus vic‐Dioxime Ligands and their Ni^II Complexes: Synthesis, Characterization and Solubility Properties

B. Guzel Faculty of Sciences and Letters, Chemistry Department, Çukurova University, Adana, TurkeyCorrespondence[email protected]

G. Avşar Faculty of Sciences and Letters, Chemistry Department, Çukurova University, Adana, Turkey

H. F. Çınkır Faculty of Sciences and Letters, Chemistry Department, Çukurova University, Adana, Turkey

New supercritical carbon dioxide s oluble ligands, N,N′‐bis(4‐trifluoromethyl phenylamino)glyoxime, N,N′‐bis(3‐trifluoromethylphenylamino)glyoxime, N,N′‐bis(3,5‐ditrifluoromethyl phenylamino)glyoxime and their Ni^II complexes have been prepared and characterized by spectroscopic methods and elemental analysis. The solubility of the synthesized ligands and their Ni^II complexes were measured at 343.15 K and 172.4 bar in supercritical carbon dioxide.

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We are grateful to Çukurova University Research Foundation for financial support (FEF2003BAP5).

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Supercritical Carbon Dioxide‐Soluble Fluorus vic‐Dioxime Ligands and their Ni^II Complexes: Synthesis, Characterization and Solubility Properties

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Supercritical Carbon Dioxide‐Soluble Fluorus vic‐Dioxime Ligands and their Ni^II Complexes: Synthesis, Characterization and Solubility Properties