Synthesis and Characterization of Titanium Mesoporous Silicate

Abstract

In this project, surfactant hegzadesil three-methyl ammonium chloride was used as a structural informant or mould for synthesis of Mesoporous silicate molecular sieves. Many of the Mesoporous titanium silicates were synthesized by adding titanium compounds to the mixture, but considerable ratio of titanium centers placed in the frame are not accessible. This disadvantage was compensated by titanium butoxide as a titanous compound after being linked to the interior surfaces of host Mesoporous. The Mesoporous silicate was synthesized by, S⁺I⁻ method, and then titanium was linked into the cavities. The structure of synthesized compound was characterized and studied by using XRD, XRF, TGA, SEM, IR techniques, and surface adsorption of nitrogen. The results showed the formation of meso structure with hexagonal cavities, high surface area, isomorphic cavities, spherical morphology, functional groups, and the amount of titanium input into the structure.

Keywords:

• Mesoporous silicate
• SEM
• surfactant hegzadesil
• techniques three-methyl ammonium chloride
• TGA
• XRD
• XRF

Notes

¹Faujasite