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Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry Volume 46, 2016 - Issue 2
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Original Articles

Syntheses and Crystal Structures of Two Inorganic–Organic Hybrid Materials: [BDMLPX]3[Mo8O26]2[H3O]2·H2O and [BIIT][HBIIT] [ClMo12O40]

Yao LiCollege of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou, P. R. China
,
Zunzhe ShuCollege of Life Science, Tarim University, Aral City, Xinjiang, P. R. China;Key Laboratory of Biological Resource Protection and Utilization of Tarim Basin, Xinjiang Production & Construction Group, Xinjiang, Aral City, Xinjiang, P. R. China
,
Qing YangCollege of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou, P. R. China
,
Yuxia ZaiCollege of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou, P. R. China
,
Chengjie MaCollege of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou, P. R. China
,
Zhipeng HuangCollege of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou, P. R. China
,
Zhongcheng YueCollege of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou, P. R. China
&
Yunyin NiuCollege of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou, P. R. ChinaCorrespondence[email protected]
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Pages 280-285 | Received 12 Nov 2013, Accepted 04 Nov 2014, Published online: 29 Sep 2015
 
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Abstract

Two novel organic–inorganic hybrid supramolecular compounds based on organoammonium cations (OACs) and polyoxomolybdates (POMs), namely, [BDMLPX]3[Mo8O26]2[H3O]2·H2O (1) [BDMLPX = di(1,2-dimethylimidazolium) p-xylene dichloride and [BIIT][HBIIT][ClMo12O40] (2) [BIIT = 1,3-bis(imidazole-3-iumyl)-2,4,6-trimethyl benzene], have been hydrothermally synthesized and characterized by single-crystal X-ray diffraction, infrared spectroscopy, and thermal gravimetric analysis. Compound 1 contains the β-[Mo8O26]4−cluster and 2 has the classical Keggin-type discrete [ClMo12O40]− anion.

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Related Research Data

CCDC 971276: Experimental Crystal Structure Determination
Source: Cambridge Crystallographic Data Centre
CCDC 971277: Experimental Crystal Structure Determination
Source: Cambridge Crystallographic Data Centre

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