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Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry Volume 21, 1991 - Issue 8
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Original Articles

Complexes of bis(Diphehyldithiophosphinato)nickel(II) with Nitrogen and Sulphur Containing Ligands

Aref A. M. Aly Chemistry Department, Faculty of Science, Assiut University, Assiut, Egypt
,
R. M. M. Mahfouz Chemistry Department, Faculty of Science, Assiut University, Assiut, Egypt
,
Mahmoud S. El-Meligy Chemistry Department, Faculty of Science, Assiut University, Assiut, Egypt
&
Amna S. A. Zidan Chemistry Department, Faculty of Science, Assiut University, Assiut, Egypt
Pages 1249-1260 | Received 06 Sep 1990, Accepted 03 Jun 1991, Published online: 23 Sep 2006
 
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Abstract

Mixed ligand complexes of bis(diphenyldithiophosphinato)nickel(II) with some azoles and morpholine (morph) having the general formula Ni (Ph2PS2)2(azole)2 or Ni (Ph2PS2)2 (morph)2 have been prepared. Displacement reactions between bis(diphenyldithiophosphinato)-nickel(II) and dithizone (H2Dz), sodium diethyIdithiocarbamate (NaEt2dtc) Or potassium cyclohexyldithiocarbanate (Cydten) produced the mixed ligand complexes Ni(Ph2PS2) (HDz), Ni (Ph2PS2) (Et2dtc) and Ni(Ph2PS2) (Cydtcn). The newly prepared compounds were characterised on the basis of their analysis, magnetic susciptibility, infrared, electronic spectra as well as thermal analysis.

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