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Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry Volume 22, 1992 - Issue 4
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Original Articles

Preparation and Characterization of Chloroacetoxy-β-Diketonatobis(Cyclopentadienyl)Titanium(IV) Complexes

Yogendra Singh Department of Chemistry, University of Delhi, Delhi, 110007, India
&
Ramesh N. Kapoor Department of Chemistry, University of Delhi, Delhi, 110007, India
Pages 415-425 | Received 21 Aug 1991, Accepted 30 Dec 1991, Published online: 23 Sep 2006
 
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Abstract

The compounds of the type [Cp2Ti(RCOCHCOR') (XCOO)] (where Cp = cyclopentad ieny 1; R = R' = CH3 or (CH3)3C; R = CH3, R' = C6H5; × = Cl2CH or Cl3C have been synthesised In aqueous medium by the reactions of [Cp2Ti (RCOCHCOR')]Cl with the sodium salts of dichloroacetic acid or trichloroacetic acid in 1:1 molar ratio. These products have been characterized on the basis of their elemental analyses, electrical conductance, magnetic measurements, and spectroscopic (IR, 1H NMR and electronic) studies.

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