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Original Articles

Preparation of Tris(β-Diketonato)Indium and Tris(β-Ketoester) Indium from the Reaction in Non-Aqueous Solution

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Pages 447-459 | Received 03 Sep 1991, Accepted 15 Jan 1992, Published online: 23 Sep 2006
 

Abstract

Anhydrous indium chloride in non-aqueous solution reacted with β-diketones (H-dik) or β-ketoesters (H-etac) in the presence of amines or sodium cyanate to give the corresponding indium chelate compounds of the type In(dik)3 or In(etac)3 in high yield, where H-dik = CH3cOCH2COCH3 (Hacac), CH3COCH2COC6H5 (Hbzac), C6H5COCH2COC6H5 (Hdbzm), and H-etac = CH3COCH2COOC2H5 (Hetac).

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