A facile synthesis of thiosemicarbazides containing the 4-antipyrinyl group under microwave irradiation in solvent-free conditions

Jian-Ping Li College of Chemistry and Environmental Science, Henan Normal University, The Key Laboratory of Environmental Pollution Control of Henan Province, Xinxiang, 453007, Henan, P.R. ChinaCorrespondence[email protected]

Peng-Zhi Zheng College of Chemistry and Environmental Science, Henan Normal University, The Key Laboratory of Environmental Pollution Control of Henan Province, Xinxiang, 453007, Henan, P.R. China

Rui-Jie Liu College of Chemistry and Environmental Science, Henan Normal University, The Key Laboratory of Environmental Pollution Control of Henan Province, Xinxiang, 453007, Henan, P.R. China

Jun-Ge Zhu College of Chemistry and Environmental Science, Henan Normal University, The Key Laboratory of Environmental Pollution Control of Henan Province, Xinxiang, 453007, Henan, P.R. China

Gui-Rong Qu College of Chemistry and Environmental Science, Henan Normal University, The Key Laboratory of Environmental Pollution Control of Henan Province, Xinxiang, 453007, Henan, P.R. China

Abstract

A simple, efficient and eco-friendly method for the synthesis of a series of thiosemicarbazides containing 4-antipyrinyl group under microwave irradiation has been reported, no solvent and catalyst was used. Five of them are new compounds.

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Acknowledgements

We gratefully acknowledge financial support of this work by the Natural Science Foundation for China (Project No. 20372018).

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A facile synthesis of thiosemicarbazides containing the 4-antipyrinyl group under microwave irradiation in solvent-free conditions

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A facile synthesis of thiosemicarbazides containing the 4-antipyrinyl group under microwave irradiation in solvent-free conditions

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