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ABSTRACT
Thermolysis and/or microwave irradiation of thiosemicarbazones gave the corresponding isothiocyanates, which on addition of either activated nitriles or aldehydes furnished various types of azines. The mechanism was discussed. The structures of products were proved by MS, IR, NMR, and elemental analyses.
GRAPHICAL ABSTRACT
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Acknowledgements
The NMR spectrometer at Florida Institute of Technology was purchased with the assistance of the US National Science Foundation (CHE 03 42251).
Disclosure statement
No potential conflict of interest was reported by the authors.
