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Journal of Sulfur Chemistry Volume 27, 2006 - Issue 2
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Original Articles

N-Chlorosuccinimide: A simple and efficient reagent for the preparation of symmetrical disulfides

Mohammed M. Hashemi Department of Chemistry, Sharif University of Technology, PO Box, 11365-9516, Tehran, IranCorrespondence[email protected]
,
Hossein Ghafuri Department of Chemistry, Sharif University of Technology, PO Box, 11365-9516, Tehran, Iran
&
Zahed Karimi-Jaberi Department of Chemistry, Sharif University of Technology, PO Box, 11365-9516, Tehran, Iran
Pages 165-167 | Received 31 Aug 2005, Published online: 23 Aug 2006
 
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Abstract

The efficient oxidative coupling of thiols to disulfides with N-chlorosuccinimide (NCS) at room temperature is described. Simple workup, economical method, high yields of products are some advantages of this method.

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Related Research Data

Metal‐Free Reagent Dependent SS and CC Homocoupling of α‐Enolic Dithioesters at Room Temperature: Direct Access to Fully Substituted Symmetrical Thiophenes via Chemoselective Paal–Knorr Approach
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Caryophyllane Thiols, Vinyl Thioethers, Di- and Bis-Sulfides: Antioxidant and Membrane Protective Activities
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