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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 178, 2003 - Issue 11
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Original Articles

Silica Gel Promoted Highly Regioselective Ring Opening of Epoxides Using NaN3 Under Solvent Free Conditions

Ali Reza Kiasat Shahid Chamran University, Ahvaz, Iran
&
Foad Kazemi Shahid Chamran University, Ahvaz, Iran
Pages 2387-2392 | Published online: 18 Jun 2010
 
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Abstract

A convenient and efficient synthesis of vicinal azidohydrin has been achieved by ring opening of epoxides using SiO2/NaN3 under solvent free conditions. The reaction is highly regioselective and afforded the corresponding products in good to excellent yields under mild and neutral reaction conditions.

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