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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 7
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Original Articles

PALLADIUM-CATALYZED CARBONYLATIVE COUPLING OF ORGANOLEAD COMPOUNDS: SYNTHESIS OF SYMMETRICAL KETONES

Suk-Ku Kang Department of Chemistry, Sungkyunkwan University, Natural Science Campus, Suwon, 400-746, Korea
,
Hyung-Chul Ryu Department of Chemistry, Sungkyunkwan University, Natural Science Campus, Suwon, 400-746, Korea
&
Sang-Chul Choi Department of Chemistry, Sungkyunkwan University, Natural Science Campus, Suwon, 400-746, Korea
Pages 1035-1039 | Accepted 08 May 2000, Published online: 09 Nov 2006
 
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Abstract

Organolead acetates can be carbonylated in the presence of Pd2(dba)3·CHCl3 (5 mol%) and NaOMe (5 equiv.) in CH3CN under atmospheric pressure of carbon monoxide at room temperature to afford symmetrical ketones.

ACKNOWLEDGMENTS

Generous financial support from KOSEF-Center for Molecular Design and Synthesis (CMDS) is gratefully acknowledged.

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