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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 7
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Original Articles

PALLADIUM-CATALYZED CROSS-COUPLING OF ORGANOLEAD(IV) TRIACETATES WITH TERMINAL ALKYNES

Suk-Ku Kang Department of Chemistry, Sungkyunkwan University, Natural Science Campus, Suwon, 440-746, Korea
,
Hyung-Chul Ryu Department of Chemistry, Sungkyunkwan University, Natural Science Campus, Suwon, 440-746, Korea
&
Sang-Ho Lee Department of Chemistry, Sungkyunkwan University, Natural Science Campus, Suwon, 440-746, Korea
Pages 1059-1064 | Accepted 08 May 2000, Published online: 09 Nov 2006
 
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Abstract

The palladium-catalyzed carbon-carbon bond formation of organolead(IV) triacetates with terminal alkynes was accomplished with Pd2(dba)3·CHCl3 (5 mol%) and CuI (10 mol%) in the presence of NaOMe (2 equiv.) in MeOH/CH3CN (1:1) at room temperature.

ACKNOWLEDGMENTS

Generous financial support from KOSEF-Center for Molecular Design and Synthesis (CMDS) is gratefully acknowledged.

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