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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 7
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Original Articles

A MILD AND EFFICIENT CLEAVAGE OF gem-DIACETATES TO ALDEHYDES BY CBr4*

T. Ramalingam Organic Chemistry Division-I, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
,
R. Srinivas Organic Chemistry Division-I, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
,
B. V. Subba Reddy Organic Chemistry Division-I, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
&
J. S. Yadav Organic Chemistry Division-I, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
Pages 1091-1095 | Received 07 Apr 2000, Published online: 09 Nov 2006
 
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Abstract

gem-Diacetates are selectively deprotected to the corresponding aldehydes in high yields by CBr4 in refluxing acetonitrile under neutral reaction conditions.

*IICT Communication No. 4491.

ACKNOWLEDGMENTS

BVS thanks CSIR, New Delhi, for the award of fellowship.

Notes

*IICT Communication No. 4491.

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Related Research Data

Nickel boride mediated chemoselective deprotection of 1,1-diacetates to aldehydes and deprotection with concomitant reduction to alcohols at ambient temperature
Source: Informa UK Limited
Nickel boride mediated chemoselective deprotection of 1,1-diacetates to aldehydes and deprotection with concomitant reduction to alcohols at ambient temperature
Source: Informa UK Limited

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