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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 10
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Original Articles

CATALYTIC OXIDATION OF THIOLS TO DISULFIDES WITH VANADYL ACETYLACETONATE (VO(ACAC)2)*

Sadagopan Raghavan Organic Division I, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
,
A. Rajender Organic Division I, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
,
Suju C. Joseph Organic Division I, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
&
Mohd. Abdul Rasheed Organic Division I, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
Pages 1477-1480 | Received 07 Jan 2000, Published online: 02 Aug 2010
 
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Abstract

Catalytic amounts of VO(acac)2 coupled with t-butylhydroperoxide chemoselectively oxidizes thiols to disulfides under mild reaction conditions and is generally useful for a wide variety of thiols.

*IICT communication No. 4400.

ACKNOWLEDGMENTS

S.R. is thankful to Dr. J.S. Yadav, Head, Org. Div. I and Dr. K.V. Raghavan, Director, I.I.C.T, for their constant support and encouragement. A.R, S.C.J., and M.A.R. are thankful to CSIR, New Delhi, for a fellowship.

Notes

*IICT communication No. 4400.

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Related Research Data

(NH4)6Mo7O24·4H2O as an Efficient, Selective, and Reusable Catalyst for the Oxidation of Thiols to Disulfides Using Potassium Bromate
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